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Fourth, (5) (4.0 g, 10.4 mmol) was mixed with CH 2 Cl 2 (30 mL), and (2) (2.2 g, 12.5 mmol), 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide hydrochloride (EDCHCl) (2.8 g, 14.6 mmol), 4-(dimethylamino)pyridine (DMAP) (1.5 g, 12.5 mmol), and triethylamine (Et 3 N) (2.9 mL, 20.8 mmol) were added into the (5) mixture under vigorous stirring at room temperature

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