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Assen, S., Agmon-Levin, N., Elkayam, O., Cervera, R., Doran, M

a feed solution of Preparation 25, 2.40 kg, 96.7 wt.%, 2.274 mol is prepared by dissolving the solid in DMSO (13.88 kg, 12.62 L) and diluting the solution with ACN (1.09 kg, 1.39 L), creating a solution of Preparation 25 (114.3 mg/mL, 0.112 M) in 90: 10 DMSO:ACN vol/vol

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